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Issue Info: 
  • Year: 

    2013
  • Volume: 

    16
Measures: 
  • Views: 

    114
  • Downloads: 

    52
Keywords: 
Abstract: 

IT IS WELL-KNOWN THAT THE PARTICLE SIZE AND MORPHOLOGY OF NANO MATERIALS HAVE A GREAT INFLUENCE ON THEIR OPTICAL AND ELECTRICAL PROPERTIES. SO, THE CONTROLLED SYNTHESIS OF THE NANOSTRUCTURE AND NANO COMPOSITE ARE VERY IMPORTANT FOR THEIR FUNDAMENTAL AND TECHNOLOGICAL APPLICATIONS [1, 2]. IN THE PRESENT WORK, SnO2 NANOPARTICLE AND SnO2/ZN2SNO4 NANO COMPOSITE HAVE BEEN SUCCESSFULLY SYNTHESIZED USING THE REFLUX METHOD. THE HEAT TREATMENT OF SnO2 AND SnO2/ZN2SNO4 PREPARED SAMPLES WERE CARRIED OUT AT 500, 900 AND 900 OC RESPECTIVELY. THE SnO2 NANOPARTICLES WERE SYNTHESIZED AT DIFFERENT PH VALUES (4, 12 AND 14). THE OBTAINED SAMPLES WERE CHARACTERIZED BY X-RAY DIFFRACTION (XRD), FOURIER TRANSFORM INFRARED SPECTROSCOPY (FT-IR) AND EMISSION SCANNING ELECTRON MICROSCOPY (FE-SEM). THE STRUCTURE OF SnO2 AND SnO2/ZN2SNO4 COMPOSITE WERE INVESTIGATED BY THE XRD EXPERIMENT. RESULTS SHOW THAT ORTHORHOMBIC, TETRAGONAL AND TETRAGONAL/CUBIC PHASE WERE OBSERVED FOR SnO2 AND SnO2/ZN2SNO4 COMPOSITE AT 500, 900 AND 900 OC RESPECTIVELY. FE-SEM REVEALED THE SnO2 PARTICLE WITH SIZES OF (31-62 NM) DEPENDING ON THE PH VALUES. THE PHOTO CATALYTIC PERFORMANCE OF SnO2 NANOPARTICLE AND SnO2/ZN2SNO4 NANO COMPOSITE WERE EVALUATED BY DECOLORIZATION OF METHYLENE BLUE AND CONGO RED SOLUTION UNDER UV-VIS IRRADIATION. THIS WORK SHOWS THE POSSIBILITY OF USING OF SnO2/ZN2SNO4 NANO COMPOSITE AS A PHOTO CATALYST FOR REMOVAL OF ANIONIC AND CATIONIC DYES. THE PHOTO CATALYTIC RESULTS SHOW THAT SnO2/ZN2SNO4 NANO COMPOSITE CAN EFFECTIVELY DEGRADE 82% METHYLENE BLUE AND 54% CONGO RED SOLUTION WITH IN 180 MIN UNDER UV-VIS IRRADIATION. SCIENCE, THE PREADSORPTION OF DYE BEFORE IRRADIATION IS VERY IMPORTANT FOR PHOTO CATALYSIS EXPERIMENTS, THE PREADSORPTON DEGREE OF DYE SOLUTION WAS MEASURED. ALSO, THE REUSABILITY OF PREPARED NANO COMPOSITE WAS INVESTIGATED THROUGH SUCCESSIVE 4 CYCLES OF EXPERIMENTS.

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Issue Info: 
  • Year: 

    2019
  • Volume: 

    38
  • Issue: 

    4
  • Pages: 

    19-26
Measures: 
  • Citations: 

    0
  • Views: 

    155
  • Downloads: 

    167
Abstract: 

Esterification reactions of some polyols and diols were investigated in the presence of SnO2 and nano-SnO2 and the results were compared with the catalyst-free conditions. High conversions were obtained for most of the reactions in the presence of SnO2 and nano-SnO2 which shows the high catalytic activity of SnO2 and nano-SnO2 for the esterification reaction. Low cost of the catalysts compared to alkyl tins, high safety compared to protic acids such as sulfuric acid and high chemical and thermal stability of the catalysts make the reactions interesting for the large-scale production of various polyol esters. Due to the important role of the polyol esters in various industries especially in the lubricant industry, the introduced approach can be interesting.

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Author(s): 

NOURI A. | FAKHRI A. | NOURI A.EZOU

Issue Info: 
  • Year: 

    2013
  • Volume: 

    10
  • Issue: 

    2
  • Pages: 

    137-142
Measures: 
  • Citations: 

    0
  • Views: 

    2335
  • Downloads: 

    173
Abstract: 

Metal oxides play a very important role in many areas of chemistry, physics and materials science. The metal elements are able to form a large diversity of oxide compounds. In this investigation, we synthesis SnO2 and C, N, S-tridoped SnO2 nanoparticles by precipitation method. The synthesized SnO2 and C, N, S-tridoped SnO2 nanoparticles were characterized by instrumental analysis methods, such as X-ray diffraction (XRD), Fourier transform infrared  spectroscopy (FTIR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) techniques. The observed results showed particle size 30 nm.

Yearly Impact: مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Author(s): 

Issue Info: 
  • Year: 

    2023
  • Volume: 

    49
  • Issue: 

    2
  • Pages: 

    2388-2393
Measures: 
  • Citations: 

    1
  • Views: 

    24
  • Downloads: 

    0
Keywords: 
Abstract: 

Yearly Impact: مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Issue Info: 
  • Year: 

    2025
  • Volume: 

    10
  • Issue: 

    2
  • Pages: 

    108-131
Measures: 
  • Citations: 

    0
  • Views: 

    9
  • Downloads: 

    0
Abstract: 

Water pollution remains a pressing environmental issue, necessitating the development of advanced photocatalysts for effective wastewater treatment. This research synthesized pure SnO2 and SnO2/Al2O3 core-shell composite photocatalysts via a simple and cost-efficient sol-gel method. The thermoluminescence (TL) glow curves were recorded after 15 minutes of X-ray irradiation and analyzed using the initial rise method, peak shape analysis, and curve fitting techniques. These analyses revealed the presence of multiple trapping sites in SnO2/Al2O3 composite, providing valuable insights into charge carrier dynamics and material properties essential for photocatalytic and radiation dosimetry applications. The photocatalytic performance of the materials was assessed by monitoring the degradation of methyl orange (MO) under UV irradiation of 254 nm wavelength. The SnO2/Al2O3 composite exhibited significantly improved photocatalytic efficiency, achieving 80.26% MO degradation within 1 hour with a rate constant of 0.03174 min⁻¹, surpassing the performance of pure SnO2. This enhanced activity is attributed to the localized surface plasmon resonance (LSPR) and abundant trapping sites of the composite, which effectively capture photogenerated charge carriers, reduce recombination rates, and maintain a higher concentration of reactive species such as hydroxyl radicals and superoxide anions. Moreover, the TL glow curve analysis highlights the potential of the SnO2/Al2O3 composite as a reliable material for radiation dosimetry, suitable for applications in medical, environmental, and industrial fields requiring accurate radiation measurements. These results underscore the dual-functional nature of the SnO2/Al2O3 composite, demonstrating its efficacy as both an efficient photocatalyst for wastewater treatment and a promising candidate for radiation monitoring.

Yearly Impact: مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Issue Info: 
  • Year: 

    2025
  • Volume: 

    5
  • Issue: 

    1
  • Pages: 

    17-22
Measures: 
  • Citations: 

    0
  • Views: 

    8
  • Downloads: 

    0
Abstract: 

In this work, the three-layer SnO2/Ag/SnO2 coating on the glass substrate was designed and the optimal thickness was calculated using Film Wizard software. Then the designed samples were fabricated using thermal evaporation technique. Analysis was conducted on optical, electrical, and thermal properties of the samples, including coefficient of merit, surface resistance, and optical transmittance and reflectance. The results showed that the three-layer structures, SnO2/Ag/SnO2, have the necessary and favorable conditions for use as heat insulating and energy saving coatings on glass windows. The optimal thickness was determined 20nm for silver and 70 nm for SnO2. The recorded optical transmission in the visible spectrum and the reflected light in the infrared spectrum are 79.66% and 88.66%, correspondingly. The surface electrical resistance of 11.69 Ω⁄sq has been obtained for the constructed system, which is a suitable value for this coating. The calculated optical values show that the heat transfer from sunlight is minimized through this coating and this coating can be used as a suitable energy storage.

Yearly Impact: مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Issue Info: 
  • Year: 

    2013
  • Volume: 

    16
Measures: 
  • Views: 

    134
  • Downloads: 

    82
Abstract: 

IN THIS RESEARCH, WE PREPARED TIO2 THIN FILMS WITH DIFFERENT MOLAR RATIOS OF SN ON SLIDE GLASS SUBSTRATE USING SPIN COATING PROCESS. AFTER ANNEALING THE SAMPLES, WE STUDIED THE SURFACE MORPHOLOGY BY SCANNING ELECTRON MICROSCOPE (SEM, S-4160 MODEL AT 15 KV). TO DETERMINE THE OPTICAL ENERGYBAND GAP, WE ALSO MEASURED THE ABSORPTION AND TRANSMISSION SPECTRA BY SPECTROPHOTOMETER (UV-VIS, PG INSTRUMENT-T80+TYPE).

Yearly Impact:   مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

View 134

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Issue Info: 
  • Year: 

    1395
  • Volume: 

    13
Measures: 
  • Views: 

    259
  • Downloads: 

    0
Keywords: 
Abstract: 

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Yearly Impact:   مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Author(s): 

Issue Info: 
  • Year: 

    2022
  • Volume: 

    138
  • Issue: 

    -
  • Pages: 

    0-0
Measures: 
  • Citations: 

    1
  • Views: 

    10
  • Downloads: 

    0
Keywords: 
Abstract: 

Yearly Impact: مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Writer: 

Ghasemi Teroujeni Seyede Mahjoube | Soleimani Esmaiel

Issue Info: 
  • Year: 

    2015
  • Volume: 

    18
Measures: 
  • Views: 

    149
  • Downloads: 

    52
Abstract: 

BACKGROUND: IN RECENT YEARS, THE SYNTHESIS AND PHYSICAL CHARACTERIZATION OF NANOSCALE SEMICONDUCTORS HAVE AROUSED MUCH INTEREST [1–3]. AMONG THESE SEMICONDUCTORS, SnO2 HAS ATTRACTED ATTENTION DUE TO ITS OPTICAL AND ELECTRONIC PROPERTIES. SnO2 IS AN IMPORTANT N-TYPE WIDE-ENERGY-GAP SEMICONDUCTOR (EG=3.6 EV), WHICH HAS A WIDE RANGE OF APPLICATIONS SUCH AS GAS SENSORS, TRANSPARENT CONDUCTING ELECTRODES [4]...

Yearly Impact:   مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

View 149

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