OPTIMIZATION OF SYNTHESIZING CONDITIONS FOR TIB2 POWDER IN ALUMINOTHERMIC PROCESSING USING THE TAGUCHI EXPERIMENTAL DESIGN

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SHAH BAHRAMI B.; SARAF MAMOURI R.; EHSANI N.

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Paper Information

Journal: JOURNAL OF FACULTY OF ENGINEERING (UNIVERSITY OF TABRIZ) Year:2006 | Volume:31 | Issue:2 (41 MECHANICS) Page(s): 59-65

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Title

OPTIMIZATION OF SYNTHESIZING CONDITIONS FOR TIB2 POWDER IN ALUMINOTHERMIC PROCESSING USING THE TAGUCHI EXPERIMENTAL DESIGN

Author(s)

SHAH BAHRAMI B. | SARAF MAMOURI R. | EHSANI N.

Keywords

TITANIUM DIBORIDE (TIB2)

SHS

ALUMINOTHERMIC

TAGUCHI EXPERIMENTAL DESIGN

Abstract

TiB2 powder was synthesized via simultaneous Aluminum reduction of TiO2 and B2O3 according to SHS reaction in an oxidation atmosphere. This method opposite to other methods, does not need to have controlled atmosphere and high temperature. In this work, TAGUCHI EXPERIMENTAL DESIGN was used and different effective parameters and their ranges were studied. Then, the related levels of experiments were determined for Taguchi method and various experiments were carried out based on the determined variation levels. Using statistical calculations, contribution percentage of each parameter was calculated and the most suitable conditions were extracted. Finally, the accuracy experiments were carried out so that the results were corresponded on what obtained from calculations. ‏The most appropriate conditions of synthesis consists of: 1170°C, 0.5 hr, Al and B2O3 powder contents 1.194 and 1.124 in stoichiometric ratio, respectively, particle size less than 44 mm for Al powder and between the range of 63 mm to 149 mm for TiO2 and B2O3 powders.

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APA: Copy

SHAH BAHRAMI, B., SARAF MAMOURI, R., & EHSANI, N.. (2006). OPTIMIZATION OF SYNTHESIZING CONDITIONS FOR TIB2 POWDER IN ALUMINOTHERMIC PROCESSING USING THE TAGUCHI EXPERIMENTAL DESIGN. JOURNAL OF FACULTY OF ENGINEERING (UNIVERSITY OF TABRIZ), 31(2 (41 MECHANICS)), 59-65. SID. https://sid.ir/paper/545625/en

Vancouver: Copy

SHAH BAHRAMI B., SARAF MAMOURI R., EHSANI N.. OPTIMIZATION OF SYNTHESIZING CONDITIONS FOR TIB2 POWDER IN ALUMINOTHERMIC PROCESSING USING THE TAGUCHI EXPERIMENTAL DESIGN. JOURNAL OF FACULTY OF ENGINEERING (UNIVERSITY OF TABRIZ)[Internet]. 2006;31(2 (41 MECHANICS)):59-65. Available from: https://sid.ir/paper/545625/en

IEEE: Copy

B. SHAH BAHRAMI, R. SARAF MAMOURI, and N. EHSANI, “OPTIMIZATION OF SYNTHESIZING CONDITIONS FOR TIB2 POWDER IN ALUMINOTHERMIC PROCESSING USING THE TAGUCHI EXPERIMENTAL DESIGN,” JOURNAL OF FACULTY OF ENGINEERING (UNIVERSITY OF TABRIZ), vol. 31, no. 2 (41 MECHANICS), pp. 59–65, 2006, [Online]. Available: https://sid.ir/paper/545625/en

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