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Title

ELECTROCHEMICAL SYNTHESIS OF PHOSPHONIUM-BASED IONIC LIQUID SUPPORTED/MWCNT/PLATINUM NANOCOMPOSITE AS AN EFFICIENT NANOELECTROCATALYST

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Abstract

 SYNERGISTIC EFFECT OF DIFFERENT INGREDIENTS INTO THE NANOCOMPOSITES CAUSED TO INTENSIVE CONCENTRATION ON THEM. AS AN EFFICIENT NANOELECTROCATALYST, PLATINUM-BASED NANOCOMPOSITE HAS BEEN ELECTROCHEMICALLY SYNTHESIZED USING MULTI-WALLED CARBON NANOTUBE (MWCNTS) IN THE PRESENCE OF PHOSPHONIUM-BASED IONIC LIQUID [P14, 6, 6, 6][N(TFMS)2A] (TRIHEXYL TETRADECYLPHOSPHONIUM BIS (TRIFLUOROMETHYLSULFONYL) AMIDE AS LINKER. APPLYING AN APPROPRIATE REDUCING POTENTIAL OR DIFFERENTIAL CURRENT PULSE IN THE QUATERNARY PHOSPHONIUM IONIC LIQUID AND MWCNTS CAUSED THE PT/MWCNT/RTIL NANOCOMPOSITE TO BE DEPOSITED ON GLASSY CARBON ELECTRODE (GCE). THE COMPARISON OF CVS WITH AND WITHOUT THE NOBLE METAL, CONFIRMS THE REDUCTION OF NOBLE METAL IONS TO ZEROVALENT METALLIC SPECIES DEPOSITED ON RTIL ON GCE. FINALLY, ELECTROCATALYTIC BEHAVIOR OF NANOCOMPOSITE-MODIFIED ELECTRODE IS INVESTIGATED FOR METHANOL ELECTROOXIDATION.

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