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Title

AN EFFICIENT AND ONE-POT PROCEDURE FOR THE SYNTHESIS OF CHIRAL ISOXAZOLIDINE VIA CATALYTIC HIGHLY ENANTIOSELECTIVE 1, 3-DIPOLAR CYCLOADDITION

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 Start Page 133 | End Page 141

Abstract

 Synthesis of enantiomerically pure isoxazolidine via an ASYMMETRIC 1, 3- dipolar cycloaddition reaction of NITRONE with electron-deficient dipolarophile was described. The process occurs at room temperature in aqueous ethanol as a green solvent and in the presence of a bidendate bis (imine) –Cu (II) triflate complex as catalyst. The reaction mechanism is discussed on the basis of the assignment of the absolute configuration of the cycloadducts.

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