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Paper Information

Journal:   IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING   SEPTEMBER 2016 , Volume 13 , Number 3; Page(s) 54 To 59.
 
Paper: 

A QUICK ROUTE FOR THE SYNTHESIS OF PMN-PZT POWDERS

 
 
Author(s):  IZADPANAHI A.*, BAGHSHAHI S., SHALBAFZADEH A.
 
* 
 
Abstract: 

In the following research, Lead magnesium niobate relaxor ferroelectric (PMN-PZT) ceramic powders were synthesized using the combustion method grand urea as the fuel for the first time. The starting materials used were lead nitrate, magnesium acetate, niobium oxide, zirconium nitrate, titanium oxide. The raw materials were first mixed using the general formula of (1-x)Pb(Mg1/3Nb2/3)O3-xPb(Zr0.52Ti0.48)O3, with  x=0.3. The synthesized powders were characterized using XRD, SEM and FTIR spectroscopy techniques. The X-ray diffraction patterns revealed that the structure of the prepared samples were tetragonal at 500,600,700 and 800oC. However, the monoclinic phase was detected in the samples calcined at 800 oC and the amount of pyrocholore phase also drastically decreased at this temperature. The band gap widths of the samples were measured via UV spectroscopy in the wave number range of 400-4000cm-1. The results show that by increasing the calcination temperature, the band gap width of the prepared samples decreases. SEM micrographs verify that by rising the calcination temperature, the structure of the prepared samples becomes more homogenous.

 
Keyword(s): PMN-PZT, COMBUSTION METHOD, UREA, ELECTRO-CERAMIC, BAND GAP WIDTH
 
 
References: 
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Citations: 
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APA: Copy

IZADPANAHI, A., & BAGHSHAHI, S., & SHALBAFZADEH, A. (2016). A QUICK ROUTE FOR THE SYNTHESIS OF PMN-PZT POWDERS. IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING, 13(3), 54-59. https://www.sid.ir/en/journal/ViewPaper.aspx?id=569658



Vancouver: Copy

IZADPANAHI A., BAGHSHAHI S., SHALBAFZADEH A.. A QUICK ROUTE FOR THE SYNTHESIS OF PMN-PZT POWDERS. IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING. 2016 [cited 2021August01];13(3):54-59. Available from: https://www.sid.ir/en/journal/ViewPaper.aspx?id=569658



IEEE: Copy

IZADPANAHI, A., BAGHSHAHI, S., SHALBAFZADEH, A., 2016. A QUICK ROUTE FOR THE SYNTHESIS OF PMN-PZT POWDERS. IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING, [online] 13(3), pp.54-59. Available: https://www.sid.ir/en/journal/ViewPaper.aspx?id=569658.



 
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