EFFECTS OF TIME, TEMPERATURE AND PRECURSOR ON SOLID STATE SYNTHESIS OF α-TCP

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ASADI TABRIZI R.; ZAMANIAN A.; HESARAKI S.

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Journal: Advanced Ceramics Progress Year:2015 | Volume:1 | Issue:1 Page(s): 36-39

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Title

EFFECTS OF TIME, TEMPERATURE AND PRECURSOR ON SOLID STATE SYNTHESIS OF α-TCP

Author(s)

ASADI TABRIZI R. | ZAMANIAN A. | HESARAKI S. | Issue Writer Certificate

Keywords

CALCIUM PHOSPHATE CEMENT

SOLID STATE SYNTHESIS

α-TRICALCIUM PHOSPHATE

MAGNESIUM

Abstract

In this study, the correlation between impurity content of reagents used (monetite and brushite both from Merck), soaking time and firing temperature in the SOLID STATE SYNTHESIS of a-tricalcium phosphate (a -TCP) has been established. Mg impurity promoted formation of b-polymorph as a second phase in the resultant product. The extension of firing operation also led to an increase in the amount of a-TCP, higher firing temperature with an Equivalent soaking time resulted in a more purely synthesized a- TCP. The amount of α and b phases at each heating program were investigated through Match software system. The highest percentage of obtained a-TCP in the resultant product with the monetite precursor containing 0.43 wt.% MAGNESIUM impurity at 1350oC and 16 hours of soaking time was about 94%.

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APA: Copy

ASADI TABRIZI, R., ZAMANIAN, A., & HESARAKI, S.. (2015). EFFECTS OF TIME, TEMPERATURE AND PRECURSOR ON SOLID STATE SYNTHESIS OF α-TCP. ADVANCED CERAMICS PROGRESS, 1(1), 36-39. SID. https://sid.ir/paper/344472/en

Vancouver: Copy

ASADI TABRIZI R., ZAMANIAN A., HESARAKI S.. EFFECTS OF TIME, TEMPERATURE AND PRECURSOR ON SOLID STATE SYNTHESIS OF α-TCP. ADVANCED CERAMICS PROGRESS[Internet]. 2015;1(1):36-39. Available from: https://sid.ir/paper/344472/en

IEEE: Copy

R. ASADI TABRIZI, A. ZAMANIAN, and S. HESARAKI, “EFFECTS OF TIME, TEMPERATURE AND PRECURSOR ON SOLID STATE SYNTHESIS OF α-TCP,” ADVANCED CERAMICS PROGRESS, vol. 1, no. 1, pp. 36–39, 2015, [Online]. Available: https://sid.ir/paper/344472/en

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