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Paper Information

Journal:   JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)   APRIL 2014 , Volume 11 , Number 2; Page(s) 289 To 295.
 
Paper: 

THREE-COMPONENT REACTION BETWEEN AMINES, CARBON DISULFIDE AND ELECTRON-DEFICIENT DERIVATIVES OF CHLOROPYRIDINE OR CHLOROBENZENE: SYNTHESIS OF 3, 6-DIAZASPIRO [4.5] DECA-2, 7, 9-TRIEN-6-IUM CHLORIDE AND DITHIOYLCARBAMATES DERIVATIVES

 
 
Author(s):  RANJBAR KARIMI REZA*, KHAJEH KHEZRI ALIYEH, ANARY ABBASINEJAD MOHAMMAD
 
* DEPARTMENT OF CHEMISTRY, FACULTY OF SCIENCE, VALI-E-ASR UNIVERSITY, 77176 RAFSANJAN, ISLAMIC REPUBLIC OF IRAN
 
Abstract: 

In this study, three-component reaction of some primary and secondary amines with carbon disulfide in the presence of electron-deficient derivatives of chloropyridine or chlorobenzene in the CH3CN as a solvent is reported. The reaction of primary amines with carbon disulfide and electron-deficient compounds of chloropyridine or chlorobenzene after 6-8 h afforded the three-component addition product. The reaction of secondary amines with carbon disulfide and electron-deficient compounds of chloropyridine or chlorobenzene after 3-4 h afforded the two-component addition product. The product (s) of reactions were purified by recrystallization or column chromatography and their structures were identified by spectroscopy techniques such as 1H-NMR, 13C-NMR, IR, UV and elemental analysis. The reactions were carried out under mild conditions and without using a catalyst.

 
Keyword(s): THREE-COMPONENT REACTION, CARBON DISULFIDE, AMINES, ELECTRON-DEFICIENT, CHLOROPYRIDINE, SPIRO COMPOUNDS
 
 
References: 
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Click to Cite.
APA: Copy

RANJBAR KARIMI, R., & KHAJEH KHEZRI, A., & ANARY ABBASINEJAD, M. (2014). THREE-COMPONENT REACTION BETWEEN AMINES, CARBON DISULFIDE AND ELECTRON-DEFICIENT DERIVATIVES OF CHLOROPYRIDINE OR CHLOROBENZENE: SYNTHESIS OF 3, 6-DIAZASPIRO [4.5] DECA-2, 7, 9-TRIEN-6-IUM CHLORIDE AND DITHIOYLCARBAMATES DERIVATIVES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 11(2), 289-295. https://www.sid.ir/en/journal/ViewPaper.aspx?id=408511



Vancouver: Copy

RANJBAR KARIMI REZA, KHAJEH KHEZRI ALIYEH, ANARY ABBASINEJAD MOHAMMAD. THREE-COMPONENT REACTION BETWEEN AMINES, CARBON DISULFIDE AND ELECTRON-DEFICIENT DERIVATIVES OF CHLOROPYRIDINE OR CHLOROBENZENE: SYNTHESIS OF 3, 6-DIAZASPIRO [4.5] DECA-2, 7, 9-TRIEN-6-IUM CHLORIDE AND DITHIOYLCARBAMATES DERIVATIVES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS). 2014 [cited 2021May11];11(2):289-295. Available from: https://www.sid.ir/en/journal/ViewPaper.aspx?id=408511



IEEE: Copy

RANJBAR KARIMI, R., KHAJEH KHEZRI, A., ANARY ABBASINEJAD, M., 2014. THREE-COMPONENT REACTION BETWEEN AMINES, CARBON DISULFIDE AND ELECTRON-DEFICIENT DERIVATIVES OF CHLOROPYRIDINE OR CHLOROBENZENE: SYNTHESIS OF 3, 6-DIAZASPIRO [4.5] DECA-2, 7, 9-TRIEN-6-IUM CHLORIDE AND DITHIOYLCARBAMATES DERIVATIVES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), [online] 11(2), pp.289-295. Available: https://www.sid.ir/en/journal/ViewPaper.aspx?id=408511.



 
 
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