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Paper Information

Journal:   IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY   SPRING-SUMMER 2005 , Volume 13 , Number 1 ; Page(s) 19 To 28.
 
Paper: 

SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX

 
 
Author(s):  HABIBI M.H.*, TANGESTANINEZHAD S., FALAH SHOJAEI A.
 
* CHEMISTRY DEPARTMENT, ISFAHAN UNIVERSITY, ISFAHAN, 81746, IRAN
 
Abstract: 

In this research N(2-chloro-phenyl)4-nitro-thiobenzamide as a ligand was synthesized. One mmol of mercury oxide was added to the solution of 1 mmol ligand in 45 ml chloroform and after 90 min the mixture through celite or BaS to remove unreacted mercury (II) compounds. The yellow crystals, which formed by slow evaporization, was separated and recrystallized from chloroform as fine yellow crystals with 87% yield and dried in vacuo. The crystal structure of above complex was determined by single crystal X-ray diffraction method. The complex crystals in a monoclinic unit cell with a = 8.2822(9), b = 12.2907(9) , c = 13.1243(13) a=90°, B = 98.729(5)°, g = 90° and Z = 2 and space group P21/c. The S-Hg-S is linear with angle of 180°.

 
Keyword(s): CRYSTAL STRUCTURE, MERCURY(II) COMPLEX, THIOBENZAMIDE
 
 
References: 
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Citations: 
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+ Click to Cite.
APA: Copy

HABIBI, M., & TANGESTANINEZHAD, S., & FALAH SHOJAEI, A. (2005). SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 13(1), 19-28. https://www.sid.ir/en/journal/ViewPaper.aspx?id=96453



Vancouver: Copy

HABIBI M.H., TANGESTANINEZHAD S., FALAH SHOJAEI A.. SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY. 2005 [cited 2021October21];13(1):19-28. Available from: https://www.sid.ir/en/journal/ViewPaper.aspx?id=96453



IEEE: Copy

HABIBI, M., TANGESTANINEZHAD, S., FALAH SHOJAEI, A., 2005. SYNTHESIS AND CRYSTAL STRUCTURE ANALYSES OF BIS[N(2-CHLORO-PHENYL) 4-NITRO- HIOBENZAMIDATO]MERCURY(II) COMPLEX. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, [online] 13(1), pp.19-28. Available: https://www.sid.ir/en/journal/ViewPaper.aspx?id=96453.



 
 
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